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CC=Collection Code: [AB2X4]=ANX Form: [cF56]=Pearson: [e d a]=Wyckoff Symbol: [Al2MgO4]=Structure Type:
***Click the ANX, Pearson or Wyckoff Symbol to find structures with that symbol***.
CC=73343 Help
TitleCluster synthesis. 33. Synthesis and characterization of PtOs5(CO)15(mue3-S)(mue-H)6, PtOs5(CO)18(mue-H)4 and PtOs4 (CO)15(mue-H)2.
AuthorsAdams, R.D.;Pompeo, M.P.;Wu, W.-G.
ReferenceInorganic Chemistry (1991) 30, 289-290
Link XRef SCOPUS Google
CompoundC15 H2 O15 Os4 Pt1 - Di-mue-hydrido-15-carbonyl-platinumtetraosmium [A15NO2P4X15] [mP148] [e35] []
Cell13.337(2), 8.809(3), 20.141(4), 90., 90.59(2), 90.
P121/C1 (14) V=2366.15
RemarksR=0.036000 :
The coordinates are those given in the paper but the atomic distances do not agree with those calculated during testing.The coordinates are probably correct.

Atom (site) Oxid. x, y, z, B, Occupancy
Pt1(4e)0
Os1(4e)0
Os2(4e)0
Os3(4e)0
Os4(4e)0
O1(4e)-2
O2(4e)-2
O3(4e)-2
O4(4e)-2
O5(4e)-2
O6(4e)-2
O7(4e)-2
O8(4e)-2
O9(4e)-2
O10(4e)-2
O11(4e)-2
O12(4e)-2
O13(4e)-2
O14(4e)-2
O15(4e)-2
C1(4e)2
C2(4e)2
C3(4e)2
C4(4e)2
C5(4e)2
C6(4e)2
C7(4e)2
C8(4e)2
C9(4e)2
C10(4e)2
C11(4e)2
C12(4e)2
C13(4e)2
C14(4e)2
C15(4e)2
H1(4e)0
H2(4e)0
0.700.870.713.001
0.840.000.632.841
0.630.100.632.831
0.760.150.752.801
0.780.230.543.561
0.690.760.858.(11
0.640.590.646.(11
0.950.770.726.(11
0.800.760.527.(11
0.040.090.587.(11
0.460.010.726.(11
0.550.860.537.(11
0.500.360.586.(11
0.830.470.787.(11
0.590.180.856.(11
0.900.000.857.(11
0.860.460.646.(11
0.690.000.439.(11
0.660.490.477.(11
0.960.280.469.(11
0.690.800.804.(11
0.660.690.673.(11
0.900.850.694.(11
0.820.850.564.(11
0.970.060.604.(11
0.530.030.694.(11
0.58-.040.565.(11
0.550.270.604.(11
0.810.350.774.(11
0.650.170.815.(11
0.850.060.815.(11
0.820.370.614.(11
0.720.080.476.(21
0.700.390.505.(11
0.890.260.498.(21
0.840.140.684.0(1
0.650.230.694.0(1

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